2013 Spring Meeting & 9th Global Congress on Process Safety
(129a) Improved Filtration Analysis Applied to Filter Press Separations
Raymond Collins, Engineering and Process Sciences,
The Dow Chemical Co., Midland, MI
A non-traditional model describing the separation of solid
particles from a liquid suspension by pressure-driven flow through a permeable
barrier has been successfully applied to the design of several filter press
applications. This flow model was derived by applying fundamental physical
principles to the unsteady, mixed-phase system represented by cake filtration
with a filter cloth. The analysis has proven suitable for operating
modes employing both constant applied pressure and constant feed flow
rate. The design procedure uses small-scale experiments
to determine a governing permeability function with a reproducible dependence on the collected volume of filtrate that is characteristic
of the properties of the solids, liquid and filter cloth. The experimental
method and various lab-scale test filters will be described, and the utility of
this method will be demonstrated for a few common, large-scale applications in
chemical processing. These include the removal of polymer fines and metal
hydroxides from wastewater, the deliquoring of biomass from a
concentrated sediment of fermentation broth, and the isolation and washing
of micron-sized solids used to manufacture energy materials.